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I'd head to the Boone/Blowing Rock area. It may take a little longer than 3 hrs from Cary, but not much. It's crammed with beautiful scenery, waterfalls and amazing views.
If you really don't want to drive that far (and I definitely would — it's worth it) then check out Hanging Rock State Park north of the Triad.
We thoroughly enjoyed our waterfall hike at South Mountain State Park. I'm sure it is quite impressive with all the rain we've seen this summer. It is quite the hike up, but SO worth it!
This may not suit your timing, but sunset on the top of Craggy Gardens near Asheville is something I could do every night. It is a short hike so you can easily make it back to the parking lot via cell phone light.
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